Local Piezoelectric Response of Polymer/Ceramic Nanocomposite Fibers

Published in Polymers, vol. 14(24), 5379 (2022) · MDPI · Open access, CC BY
DOI: 10.3390/polym14245379

Summary

Adding ceramic BaTiO3 nanoparticles to PVDF nanofibres is a common way to raise piezoelectric response, but measuring what the composite actually does at the level of a single fibre is another matter. This study maps the effective converse piezoelectric coefficient d33,eff on individual nanocomposite fibres using piezoresponse force microscopy in constant-excitation frequency-modulation mode, a variant specifically suited to compliant materials that would be distorted by conventional contact methods. Mapping single fibres rather than whole mats shows how the ceramic inclusions actually distribute their effect along the fibre.

Authors & Affiliations

  • Andrea Magnani
    Dipartimento di Fisica "Enrico Fermi", University of Pisa, Italy
  • Simone Capaccioli
    Dipartimento di Fisica "Enrico Fermi", University of Pisa, Italy
  • Bahareh Azimi
    Department of Civil and Industrial Engineering (DICI), University of Pisa, Italy
  • Serena Danti
    Department of Civil and Industrial Engineering (DICI), University of Pisa, Italy
  • Massimiliano Labardi Corresponding
    CNR-IPCF, Pisa Unit, Italy

Linari Electrospinning Systems

Linari electrospinning system with rotating collector
The nanocomposite fibres were spun on a Linari Engineering S.r.l. system (Pisa, Italy) with the collector placed 15 cm from the needle tip under positive potential - the arrangement of our complete stations, whose high voltage control unit is coded HVG-CONT-LCD.

Topics

Piezoelectric Nanofibers Polymer/Ceramic Composites Piezoresponse Force Microscopy Single-Fiber Characterization

Materials

PVDF Barium titanate (BaTiO3)
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