Light-assisted electrospinning monitoring for soft polymeric nanofibers

Published in Scientific Reports, vol. 10 (2020) · Nature Portfolio · Open access, CC BY
DOI: 10.1038/s41598-020-73252-4

Summary

This work introduces an optical method for following the electrospinning process as it happens, addressing the difficulty of keeping fibre quality reproducible from run to run. An optical fibre is threaded through the inner channel of a coaxial needle while the polymer solution (PEO in water) is fed through the outer one: light leaving the fibre crosses the droplet at the needle tip and couples into the jet as it travels towards the collector. Numerical and analytical models were built to establish whether the coupling was feasible and robust, and experiments then showed how the process parameters govern both the waveguide length of the electrospun fibre and the diameter distribution of the resulting nanofibres. The approach turns the jet itself into a sensing element, opening the way to closed-loop monitoring of soft polymeric nanofibre production.

Authors & Affiliations

  • Dario Lunni
    Center for Micro-BioRobotics, Istituto Italiano di Tecnologia, Pontedera, Italy
  • Goffredo Giordano
    Center for Micro-BioRobotics, Istituto Italiano di Tecnologia, Pontedera, Italy
  • Francesca Pignatelli
    Center for Micro-BioRobotics, Istituto Italiano di Tecnologia, Pontedera, Italy
  • Carlo Filippeschi
    Center for Micro-BioRobotics, Istituto Italiano di Tecnologia, Pontedera, Italy
  • Stefano Linari
    Linari Engineering S.r.l., Via Umberto Forti 24/14, 56121 Pisa, Italy
  • Edoardo Sinibaldi Corresponding
    Center for Micro-BioRobotics, Istituto Italiano di Tecnologia, Pontedera, Italy
  • Barbara Mazzolai Corresponding
    Center for Micro-BioRobotics, Istituto Italiano di Tecnologia, Pontedera, Italy

Linari Electrospinning Systems

RT Advanced with coaxial needles
The study was carried out on an RT Advanced system (Linari Engineering S.r.l., Pisa, Italy) using coaxial needles, which made it possible to feed the optical fibre through the inner channel while spinning the solution from the outer one. Linari Engineering is a co-author of this publication.

Topics

Process Monitoring Coaxial Electrospinning Optical Waveguides Fiber Diameter Control

Materials

Poly(ethylene oxide) (PEO) Optical fiber
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