Production of Irregularly Shaped True-To-Life Microplastics with Embedded Optical Labels

Published in Environmental Science & Technology (2025) · American Chemical Society · Open access, CC BY
DOI: 10.1021/acs.est.5c08586

Summary

Research on microplastics is hampered by the particles used to study them: neat spheres that bear little resemblance to the irregular fragments and fibres actually found in the environment. This work proposes electrospun microfibres as a precursor material, allowing optical labels to be embedded directly during production and then broken down into irregular fragments and fibres that mimic real debris. Using polystyrene as a model polymer, the fibres were doped with organic fluorophores, giving particles that are both realistic in shape and traceable in biological and environmental experiments - two properties that were previously difficult to obtain together.

Authors & Affiliations

  • Anna J. Wieberneit
    Institute of Analytical Chemistry, Chemo- and Biosensors, University of Regensburg, Germany
  • Sebastian J. Baumann
    Institute of Analytical Chemistry, Chemo- and Biosensors, University of Regensburg, Germany
  • Hannah Triebel
    Institute of Physiology, University of Regensburg, Germany
  • Sarah Dietrich
    Institute of Analytical Chemistry, Chemo- and Biosensors, University of Regensburg, Germany
  • Nongnoot Wongkaew
    Institute of Analytical Chemistry, Chemo- and Biosensors, University of Regensburg, Germany
  • Hayo Castrop
    Institute of Physiology, University of Regensburg, Germany
  • Antje J. Baeumner Corresponding
    Institute of Analytical Chemistry, Chemo- and Biosensors, University of Regensburg, Germany

Linari Electrospinning Systems

Rotary drum system by Linari NanoTech
The microfibres were spun with a rotary drum system (Linari NanoTech) at a flow rate of 30 µl/min through a four-needle holder - a rotating collector combined with a multi-needle emitter, the configuration used when a larger quantity of fibre is needed.

Topics

Microplastics Environmental Analysis Fluorescent Labelling Reference Materials

Materials

Polystyrene Organic fluorophores
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